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EFFECTS OF ETHYLENE GLYCOL SATURATION PROTOCOLS ON XRD PATTERNS: A CRITICAL REVIEW AND DISCUSSION

¹ UMR CNRS 7566 G2R, UHP, BP 239, 54506 Vanduvre-lès-Nancy, France
² UMR CNRS 7569 LEM, INPL, BP 40, 54501 Vanduvre-lès-Nancy, France

View larger version (30K): [in a new window]   Figure 1. XRD patterns of the K-saturated material noted ‘A’: (a) heating overnight at 110°C and solvated with ethylene glycol vapor at room temperature (K-110°C-EG vapor-rt); (b) solvated with ethylene glycol vapor at room temperature (K-EG vapor-rt); (c) solvated with ethylene glycol vapor at 65°C (K-EG vapor-65°C); (d) solvated with liquid ethylene glycol; (e) air-dried (K-sat-AD). Index of reflections corresponds to dhkl in Å.

View larger version (24K): [in a new window]   Figure 2. XRD patterns of the air-dried Mg-saturated material B (Mg-sat AD), solvated with ethylene glycol vapor for 24 h at room temperature (Mg-sat EG vapor-rt) and solvated with ethylene glycol liquid (Mg-sat EG liq). Index of reflections corresponds to dhkl in Å.